纳米Fe2O3修饰涂碳型硫酸沙丁胺醇选择电极的研制与应用 |
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基金项目:辽宁省大学生科技创新项目(201510160000059);锦州医科大学大学生科技创新项目(2014D17) |
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中文摘要:制备了以纳米Fe2O3为修饰剂的涂碳型硫酸沙丁胺醇选择电极,采用电位分析方法对其各项性能进行测定。结果表明,该纳米Fe2O3修饰电极有很好的能斯特响应,其线性范围为1.0×10-6~ 0.1 mol/L,级差电位为59 mV/pC,与普通电极相比,响应时间较短(10 s),检出限更低(2.8×10-7 mol/L)。将修饰电极应用于猪肉样品中硫酸沙丁胺醇含量的测定,结果与标准方法结果相符。 |
中文关键词:纳米Fe2O3 硫酸沙丁胺醇 测定 电极 猪肉 |
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Preparation and Application of Carbon Coated Polyvinyl Chloride Membrane Salbutamol Sulfate Selective Electrode Modified with Nano-Fe2O3 |
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Abstract:A potentiometric method was developed for the determination of salbutamol sulfate by using a novel carbon coated polyvinyl chloride membrane salbutamol sulfate selective electrode modified with nano-Fe2O3.The prepared electrode showed a good Nernst response in the linear range of 1.0×10-6-0.1 mol/L with a slope of 59 mV/pC.Compared to the unmodified electrode,the electrode modified with nano-Fe2O3 exhibited a faster response time(10 s) and a lower detection limit(2.8×10-7 mol/L).The modified electrode was applied in the determination of salbutamol sulfate in pork samples, and the results were in agreement with those obtained by the standard method. |
Key Words:nano-Fe2O3 salbutamol sulfate determination electrode pork |
引用本文:张静,窦月,岳京立.纳米Fe2O3修饰涂碳型硫酸沙丁胺醇选择电极的研制与应用[J].分析测试学报,2017,36(7):887-891. |
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