Analysis of Volatile Compositions in Leaves of Cortex Magnoliae Officinalis by GC-MS and Chemometrics Methods
  
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DOI:10.3969/j.issn.1004-4957.年份.月份
KeyWord:Cortex Magnoliae Officinalis leaves  essential oil  gas chromatography-mass spectrometry(GC-MS)  heuristic evolving latent projections  selective ion analysis
  
AuthorInstitution
蒋军辉,徐小娜,杨慧仙,陈云生,谭琰 1.南华大学化学化工学院;2.南华大学公共卫生学院
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Abstract:
      Volatile components of Cortex Magnoliae Officinalis leaves from Hunan were extracted by steam distillation and analyzed by gas chromatography-mass spectrometry combined with chemometrics methods,namely heuristic evolving latent projections and selective ion analysis.Temperature-programmed retention indices were used to improve the reliability of qualitative analysis.Total 54 compounds were identified,accounting for 84.95% of the total content of volatile ingredients of the studied sample.The major constituents are alpha-,beta- and gamma-eudesmol,which account for 13.10%,28.21% and 14.67%,respectively.In addition,there are seven compounds with relatively high contents,e.g.alpha-pinene(2.96%),linalool(1.71%),paeonol(1.88%),caryophyllene(2.04%),eremophilene(3.60%),alpha-selinene(3.84%) and 1,1,4,7-tetramethyl-1A,2,3,4,4A,5,6,7B-octahydro-1H-cyclopropa[E]azulene(1.34%).The results indicated that employing chemometric methods in the analysis of the volatile chemical components in Chinese traditional medicines can greatly enhance the accuracy of qualitative analysis.The results obtained is helpful to the plant resources- exploitation and utilization of Cortex Magnoliae Officinalis.
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